Smaller crowds of protesters in the Mong Kok district set fire to barricades and riot police unleashed 2020's first volleys of tear gas in response.
Police will deploy more than 6,000 officers to deal with potential unrest over the New Year's period, according to the South China Morning Post newspaper, citing unnamed sources.
Thousands of protesters, many wearing masks and reindeer horns, gathered on the streets after scuffles in shopping malls on Christmas Eve. The protests against China's control over the territory are now in their seventh month.
Sanctions will apply to NGOs that had acted "badly" over the recent unrest in Hong Kong, China's foreign ministry spokeswoman Hua Chunying said, including the National Endowment for Democracy, Human Rights Watch and Freedom House.
The Polytechnic University stand-off is one of the more dramatic episodes in six months of unrest that began in June with protests over an extradition bill seen by many in Hong Kong as an erosion of freedoms.
Protests against the government switched from violent to peaceful as the city prepared for local elections. Protesters are now weighing their next move as city leader Carrie Lam refuses to compromise.
US President Trump, speaking on Fox News Channel's "Fox & Friends," says he had saved the restive autonomous city from being destroyed by persuading Chinese president against troop deployment there.
At least a few dozen were believed to still be at Hong Kong Polytechnic University on Thursday morning. Meanwhile, US President Donald Trump is expected to sign legislation in support of the protesters.
Dozens of students still remain holed up in the besieged Hong Kong Polytechnic University, while the US Senate voted to back Hong Kong.
The legislation is aimed at protecting human rights in Hong Kong amid China's crackdown on a pro-democracy protest movement.
City leader Carrie Lam said 600 people had left the Hong Kong Polytechnic campus, including 200 who are under 18-years-old.
Hong Kong protests started on March 31 over an extradition bill show no signs of abating, despite promises by the chief executive to withdraw the bill. Meanwhile, China seems adamant not to give in to the protesters' demands.
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